TA Instruments

AR1767-0001f

28/03/2013 08:41:03

Sample name	DI 40 mm AL P60B 10 mm gap
Sample notes	 
Experiment notes	DI Deionised water, 40 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	mr1
Sample density	1.000 g/cm^3
Results file name	AR1767
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	28/03/2013 08:41:03

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	40 mm ETC AL plate with studs
Geometry notes	Standard ETC AL parallel plate with studs
Geometry material	Aluminum
Parallel plate diameter	40.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	2.056 micro N.m.s^2
Geometry compliance	3.130E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	2.000 
Shear stress factor	79580 1/m^3
Measurement system factor	39790 1/m^3
Fluid density factor	8.378E-10 m^5
Normal force factor	1592 1/m^2
Backoff distance	26500 micro m
Approximate sample volume	12.57 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	1
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.01 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0000	6.307	2.3234	10000	20.0	5.914	31.000	0.1849	12.61	0.01466	9412	5.8423	59.15	11.685	1168.5	3.411E-3	0.0	0.5
2.0000	9.872	13.358	10000	20.0	5.916	32.000	1.063	19.74	0.05384	9415	13.4865	24.15	26.973	2697.3	3.411E-3	0.0	0.5
3.0080	15.49	25.895	10000	20.0	5.911	33.008	2.061	30.98	0.06651	9408	27.3341	9.802	54.668	5466.8	3.411E-3	0.1	0.6
4.0120	18.43	33.883	10000	20.0	5.911	34.012	2.696	36.85	0.07317	9407	41.1621	6.927	82.324	8232.4	3.411E-3	0.1	0.6
4.9960	24.67	53.880	10000	20.0	5.910	34.996	4.288	49.33	0.08691	9405	67.9811	3.864	135.96	13596	3.411E-3	0.1	0.6
6.0040	31.57	81.865	10000	20.0	5.906	36.004	6.515	63.14	0.1032	9400	106.8520	2.357	213.70	21370	3.411E-3	0.1	0.6
7.0160	34.02	91.859	10000	20.0	5.905	37.016	7.310	68.03	0.1074	9398	126.4970	2.031	252.99	25299	3.411E-3	0.1	0.6
8.0120	39.29	118.54	10000	20.0	5.901	38.012	9.433	78.59	0.1200	9391	165.4490	1.521	330.90	33090	3.411E-3	0.1	0.6
9.0160	46.02	155.43	10000	20.0	5.895	39.016	12.37	92.04	0.1344	9382	225.0220	1.107	450.04	45004	3.411E-3	0.2	0.7
10.000	50.94	185.79	10000	20.0	5.887	40.000	14.78	101.9	0.1451	9369	274.8090	0.9028	549.62	54962	3.411E-3	0.2	0.7
10.996	55.70	219.39	10000	20.0	5.880	40.996	17.46	111.4	0.1567	9359	327.7630	0.7540	655.53	65553	3.411E-3	0.2	0.7
12.016	60.08	251.92	10000	20.0	5.870	42.016	20.05	120.2	0.1668	9342	377.5720	0.6471	755.14	75514	3.411E-3	0.2	0.7
13.016	64.39	287.43	10000	20.0	5.863	43.016	22.87	128.8	0.1776	9331	434.7570	0.5627	869.51	86951	3.411E-3	0.2	0.7
14.000	69.13	328.56	10000	20.0	5.850	44.000	26.15	138.3	0.1891	9310	498.5920	0.4870	997.18	99719	3.411E-3	0.2	0.7
15.000	75.66	392.06	10000	20.0	5.838	45.000	31.20	151.3	0.2062	9292	596.0370	0.4058	1192.1	1.1921E5	3.411E-3	0.3	0.8
16.004	79.91	432.20	10000	20.0	5.826	46.004	34.39	159.8	0.2152	9272	664.1220	0.3630	1328.2	1.3282E5	3.411E-3	0.3	0.8
17.000	84.51	484.32	10000	20.0	5.818	47.000	38.54	169.0	0.2280	9260	741.3430	0.3242	1482.7	1.4827E5	3.411E-3	0.3	0.8
18.016	90.96	548.89	10000	20.0	5.793	48.016	43.68	181.9	0.2401	9220	854.9410	0.2786	1709.9	1.7099E5	3.412E-3	0.3	0.8
19.000	95.01	600.20	10000	20.0	5.785	49.000	47.76	190.0	0.2513	9207	931.0910	0.2550	1862.2	1.8622E5	3.411E-3	0.3	0.8
20.000	99.39	649.35	10000	20.0	5.769	50.000	51.67	198.8	0.2600	9182	1020.0600	0.2324	2040.1	2.0401E5	3.411E-3	0.3	0.8
21.000	105.8	727.77	10000	20.0	5.743	51.000	57.91	211.6	0.2737	9141	1153.2800	0.2041	2306.6	2.3066E5	3.411E-3	0.4	0.9
22.020	109.9	778.23	10000	20.0	5.730	52.020	61.93	219.8	0.2818	9119	1242.0601	0.1888	2484.1	2.4841E5	3.411E-3	0.4	0.9
23.012	114.2	827.44	10000	20.0	5.705	53.012	65.85	228.5	0.2882	9079	1343.5300	0.1740	2687.1	2.6871E5	3.412E-3	0.4	0.9
24.000	120.6	922.50	10000	20.0	5.681	54.000	73.41	241.3	0.3043	9042	1495.5900	0.1553	2991.2	2.9912E5	3.411E-3	0.4	0.9
25.016	124.7	977.06	10000	20.0	5.657	55.016	77.75	249.4	0.3117	9003	1597.6500	0.1447	3195.3	3.1953E5	3.411E-3	0.4	0.9
26.000	129.1	1042.0	10000	20.0	5.643	56.000	82.92	258.1	0.3213	8981	1710.9301	0.1348	3421.9	3.4219E5	3.411E-3	0.4	0.9
27.016	135.4	1151.2	10000	20.0	5.617	57.016	91.61	270.9	0.3382	8940	1881.8700	0.1218	3763.7	3.7637E5	3.411E-3	0.5	1.0
28.012	139.5	1217.3	10000	20.0	5.595	58.012	96.87	279.1	0.3471	8905	1995.8500	0.1143	3991.7	3.9917E5	3.411E-3	0.5	1.0
29.012	143.6	1280.9	10000	20.0	5.565	59.012	101.9	287.3	0.3548	8857	2116.0100	0.1073	4232.0	4.2320E5	3.411E-3	0.5	1.0
30.000	150.0	1386.9	10000	20.0	5.524	60.000	110.4	300.1	0.3678	8792	2305.8501	0.09764	4611.7	4.6117E5	3.411E-3	0.5	1.0
31.000	154.1	1466.1	10000	20.0	5.500	61.000	116.7	308.3	0.3785	8753	2437.4299	0.09211	4874.9	4.8749E5	3.411E-3	0.5	1.0
32.000	158.2	1536.1	10000	20.0	5.473	62.000	122.2	316.5	0.3862	8711	2565.0200	0.08696	5130.0	5.1300E5	3.411E-3	0.5	1.0
33.000	164.6	1668.5	10000	20.0	5.448	63.000	132.8	329.3	0.4032	8671	2775.3401	0.07997	5550.7	5.5507E5	3.411E-3	0.6	1.1
34.000	168.8	1741.5	10000	20.0	5.443	64.000	138.6	337.6	0.4105	8662	2912.5400	0.07601	5825.1	5.8251E5	3.411E-3	0.6	1.1
35.000	174.9	1871.9	10000	20.0	5.379	65.000	149.0	349.7	0.4259	8560	3127.7300	0.06999	6255.5	6.2555E5	3.411E-3	0.6	1.1
36.000	179.1	1937.6	10000	20.0	5.352	66.000	154.2	358.2	0.4304	8518	3280.1101	0.06638	6560.2	6.5602E5	3.411E-3	0.6	1.1
36.996	183.2	2021.0	10000	20.0	5.301	66.996	160.8	366.5	0.4388	8436	3433.4600	0.06281	6866.9	6.8669E5	3.411E-3	0.6	1.1
38.004	189.3	2160.8	10000	20.0	5.272	68.004	171.9	378.6	0.4542	8391	3658.9199	0.05855	7317.8	7.3178E5	3.411E-3	0.6	1.1
39.000	193.5	2240.6	10000	20.0	5.241	69.000	178.3	386.9	0.4608	8341	3824.0200	0.05572	7648.0	7.6480E5	3.411E-3	0.7	1.2
40.000	199.7	2359.9	10000	20.0	5.199	70.000	187.8	399.3	0.4703	8275	4068.3401	0.05189	8136.7	8.1367E5	3.411E-3	0.7	1.2
41.012	203.7	2448.4	10000	20.0	5.143	71.012	194.8	407.4	0.4783	8186	4233.0298	0.04933	8466.1	8.4661E5	3.411E-3	0.7	1.2
42.012	210.0	2550.9	10000	20.0	5.074	72.012	203.0	419.9	0.4834	8075	4498.8701	0.04580	8997.7	8.9977E5	3.411E-3	0.7	1.2
43.004	214.1	2713.6	10000	20.0	5.082	73.004	215.9	428.1	0.5044	8088	4675.7300	0.04413	9351.5	9.3515E5	3.411E-3	0.7	1.2
43.996	218.1	2808.0	10000	20.0	5.068	73.996	223.5	436.2	0.5122	8066	4851.0200	0.04238	9702.0	9.7020E5	3.411E-3	0.7	1.2
45.012	224.2	2962.3	10000	20.0	4.987	75.012	235.7	448.5	0.5256	7937	5128.7998	0.03946	10258	1.0258E6	3.411E-3	0.8	1.3
46.012	228.4	3068.4	10000	20.0	4.994	76.012	244.2	456.8	0.5345	7949	5317.9902	0.03809	10636	1.0636E6	3.411E-3	0.8	1.3
47.012	234.5	3230.1	10000	20.0	4.912	77.012	257.0	469.0	0.5481	7817	5602.8501	0.03555	11206	1.1206E6	3.411E-3	0.8	1.3
48.016	238.5	3318.1	10000	20.0	4.872	78.016	264.0	477.0	0.5535	7753	5798.4600	0.03407	11597	1.1597E6	3.411E-3	0.8	1.3
49.012	242.6	3430.6	10000	20.0	4.819	79.012	273.0	485.3	0.5626	7669	6001.5000	0.03257	12003	1.2003E6	3.411E-3	0.8	1.3
50.012	248.8	3586.2	10000	20.0	4.772	80.012	285.4	497.5	0.5736	7595	6306.4302	0.03068	12613	1.2613E6	3.411E-3	0.8	1.3
50.996	252.8	3709.0	10000	20.0	4.722	80.996	295.2	505.6	0.5838	7515	6510.1099	0.02940	13020	1.3020E6	3.411E-3	0.8	1.3
52.000	259.0	3873.8	10000	20.0	4.684	82.000	308.3	518.0	0.5951	7455	6831.7100	0.02779	13663	1.3663E6	3.411E-3	0.9	1.4
53.004	263.1	3975.4	10000	20.0	4.590	83.004	316.3	526.2	0.6012	7306	7046.0801	0.02638	14092	1.4092E6	3.411E-3	0.9	1.4
54.016	269.1	4150.0	10000	20.0	4.560	84.016	330.2	538.3	0.6135	7257	7374.1401	0.02505	14748	1.4748E6	3.411E-3	0.9	1.4
54.996	273.3	4266.2	10000	20.0	4.529	84.996	339.5	546.5	0.6212	7207	7604.0698	0.02413	15208	1.5208E6	3.411E-3	0.9	1.4
56.000	277.3	4440.3	10000	20.0	4.543	86.000	353.3	554.6	0.6371	7230	7827.9399	0.02350	15656	1.5656E6	3.411E-3	0.9	1.4
57.012	283.4	4556.6	10000	20.0	4.391	87.012	362.6	566.7	0.6398	6989	8170.1699	0.02176	16340	1.6340E6	3.411E-3	1.0	1.5
58.012	287.4	4718.3	10000	20.0	4.319	88.012	375.5	574.9	0.6531	6874	8409.8701	0.02080	16820	1.6820E6	3.411E-3	1.0	1.5
59.012	293.6	4937.9	10000	20.0	4.312	89.012	392.9	587.2	0.6692	6863	8767.2803	0.01990	17535	1.7535E6	3.411E-3	1.0	1.5
60.012	297.6	5042.0	10000	20.0	4.214	90.012	401.2	595.1	0.6742	6707	9006.7695	0.01894	18014	1.8014E6	3.411E-3	1.0	1.5

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0120	300.0	5150.5	10000	20.0	4.310	91.012	409.9	600.0	0.6831	6860	304.7070	0.01905	609.41	60941	3.411E-3	0.0	1.5
2.0080	300.0	5138.1	10000	20.0	4.204	92.008	408.9	600.0	0.6815	6691	556.3960	0.01859	1112.8	1.1128E5	3.411E-3	0.0	1.5
2.9920	300.0	5082.0	10000	20.0	4.199	92.992	404.4	600.0	0.6740	6683	809.4760	0.01857	1619.0	1.6190E5	3.411E-3	0.0	1.5
4.0080	300.0	5115.4	10000	20.0	4.170	94.008	407.1	600.0	0.6785	6637	1184.2700	0.01844	2368.5	2.3685E5	3.411E-3	0.1	1.6
5.0080	300.0	5116.6	10000	20.0	4.229	95.008	407.2	600.1	0.6785	6731	1435.6500	0.01869	2871.3	2.8713E5	3.411E-3	0.1	1.6
5.9920	300.0	5123.5	10000	20.0	4.227	95.992	407.7	600.0	0.6795	6727	1816.3000	0.01869	3632.6	3.6326E5	3.411E-3	0.1	1.6
7.0080	300.0	5102.5	10000	20.0	4.173	97.008	406.0	600.0	0.6767	6642	2063.8701	0.01845	4127.7	4.1277E5	3.411E-3	0.1	1.6
7.9920	300.0	5117.4	10000	20.0	4.194	97.992	407.2	600.0	0.6787	6675	2315.2100	0.01854	4630.4	4.6304E5	3.411E-3	0.1	1.6
9.0080	300.0	5131.7	10000	20.0	4.278	99.008	408.4	599.9	0.6807	6809	2692.2800	0.01892	5384.6	5.3846E5	3.411E-3	0.2	1.7
9.9920	300.0	5147.5	10000	20.0	4.186	99.992	409.6	600.0	0.6827	6663	2945.9800	0.01851	5892.0	5.8920E5	3.411E-3	0.2	1.7
11.012	300.0	5096.5	10000	20.0	4.195	101.012	405.6	600.0	0.6759	6677	3194.8501	0.01854	6389.7	6.3897E5	3.411E-3	0.2	1.7
12.008	300.0	5120.6	10000	20.0	4.246	102.008	407.5	600.0	0.6792	6758	3571.8899	0.01877	7143.8	7.1438E5	3.411E-3	0.2	1.7
13.008	300.0	5141.0	10000	20.0	4.237	103.008	409.1	600.0	0.6818	6744	3823.2200	0.01873	7646.4	7.6464E5	3.411E-3	0.2	1.7
14.012	300.0	5095.6	10000	20.0	4.176	104.012	405.5	600.0	0.6758	6646	4200.2300	0.01846	8400.5	8.4005E5	3.411E-3	0.2	1.7
14.996	300.0	5107.4	10000	20.0	4.209	104.996	406.4	600.0	0.6774	6699	4451.5400	0.01861	8903.1	8.9031E5	3.411E-3	0.2	1.7
15.992	300.0	5113.7	10000	20.0	4.159	105.992	406.9	600.0	0.6782	6619	4704.4800	0.01839	9409.0	9.4090E5	3.411E-3	0.3	1.8
16.992	300.0	5077.4	10000	20.0	4.192	106.992	404.0	600.0	0.6734	6671	5079.8799	0.01853	10160	1.0160E6	3.411E-3	0.3	1.8
18.008	300.0	5144.4	10000	20.0	4.190	108.008	409.4	600.0	0.6822	6668	5332.3901	0.01852	10665	1.0665E6	3.411E-3	0.3	1.8
19.008	300.0	5107.0	10000	20.0	4.230	109.008	406.4	600.0	0.6773	6732	5708.4302	0.01870	11417	1.1417E6	3.411E-3	0.3	1.8
19.992	300.0	5091.2	10000	20.0	4.184	109.992	405.1	600.0	0.6753	6660	5959.7598	0.01850	11920	1.1920E6	3.411E-3	0.3	1.8
21.012	300.0	5068.9	10000	20.0	4.167	111.012	403.4	600.1	0.6722	6632	6210.7500	0.01842	12422	1.2422E6	3.411E-3	0.4	1.9
22.008	300.0	5089.8	10000	20.0	4.186	112.008	405.0	600.0	0.6750	6663	6587.9902	0.01851	13176	1.3176E6	3.411E-3	0.4	1.9
23.008	300.0	5075.8	10000	20.0	4.197	113.008	403.9	600.1	0.6731	6680	6840.8301	0.01855	13682	1.3682E6	3.411E-3	0.4	1.9
24.008	300.0	5113.8	10000	20.0	4.191	114.008	406.9	600.0	0.6782	6670	7217.6802	0.01853	14435	1.4435E6	3.411E-3	0.4	1.9
25.008	300.0	5147.3	10000	20.0	4.193	115.008	409.6	600.0	0.6827	6673	7467.5698	0.01854	14935	1.4935E6	3.411E-3	0.4	1.9
25.992	300.0	5143.1	10000	20.0	4.220	115.992	409.3	600.0	0.6821	6716	7718.7002	0.01866	15437	1.5437E6	3.411E-3	0.4	1.9
27.008	300.0	5144.1	10000	20.0	4.299	117.008	409.4	600.0	0.6823	6842	8097.4702	0.01901	16195	1.6195E6	3.411E-3	0.5	2.0
27.992	300.0	5087.3	10000	20.0	4.178	117.992	404.8	600.0	0.6747	6649	8348.3896	0.01847	16697	1.6697E6	3.411E-3	0.5	2.0
28.992	300.0	5140.6	10000	20.0	4.193	118.992	409.1	600.0	0.6818	6674	8598.5596	0.01854	17197	1.7197E6	3.411E-3	0.5	2.0
30.008	300.0	5101.9	10000	20.0	4.172	120.008	406.0	600.0	0.6767	6641	8976.6904	0.01845	17953	1.7953E6	3.411E-3	0.5	2.0
30.992	300.0	5145.2	10000	20.0	4.169	120.992	409.4	600.0	0.6825	6636	9226.6104	0.01844	18453	1.8453E6	3.411E-3	0.5	2.0
31.992	300.0	5120.6	10000	20.0	4.219	121.992	407.5	600.0	0.6792	6715	9604.0098	0.01865	19208	1.9208E6	3.411E-3	0.5	2.0
33.008	300.0	5103.8	10000	20.0	4.215	123.008	406.1	600.0	0.6770	6709	9854.9502	0.01864	19710	1.9710E6	3.411E-3	0.6	2.1
33.992	300.0	5101.8	10000	20.0	4.194	123.992	406.0	600.0	0.6766	6675	10106.500	0.01854	20213	2.0213E6	3.411E-3	0.6	2.1
35.008	300.0	5117.5	10000	20.0	4.265	125.008	407.2	600.0	0.6787	6788	10483.400	0.01886	20967	2.0967E6	3.411E-3	0.6	2.1
36.012	300.0	5091.4	10000	20.0	4.156	126.012	405.2	600.0	0.6753	6614	10734.800	0.01837	21470	2.1470E6	3.411E-3	0.6	2.1
36.996	300.0	5121.5	10000	20.0	4.210	126.996	407.6	600.0	0.6793	6700	11113.000	0.01861	22226	2.2226E6	3.411E-3	0.6	2.1
37.992	300.0	5138.8	10000	20.0	4.200	127.992	408.9	600.0	0.6816	6684	11367.300	0.01857	22735	2.2735E6	3.411E-3	0.6	2.1
39.008	300.0	5121.3	10000	20.0	4.212	129.008	407.5	600.0	0.6792	6704	11614.200	0.01862	23228	2.3228E6	3.411E-3	0.7	2.2
39.992	300.0	5120.9	10000	20.0	4.227	129.992	407.5	600.0	0.6792	6727	11991.400	0.01869	23983	2.3983E6	3.411E-3	0.7	2.2
41.016	300.0	5102.9	10000	20.0	4.202	131.016	406.1	600.0	0.6768	6687	12242.600	0.01858	24485	2.4485E6	3.411E-3	0.7	2.2
42.008	300.0	5091.4	10000	20.0	4.236	132.008	405.2	600.1	0.6752	6741	12622.100	0.01872	25244	2.5244E6	3.411E-3	0.7	2.2
43.008	300.0	5126.3	10000	20.0	4.232	133.008	407.9	600.0	0.6799	6735	12871.100	0.01871	25742	2.5742E6	3.411E-3	0.7	2.2
44.008	300.0	5115.5	10000	20.0	4.196	134.008	407.1	600.0	0.6784	6678	13122.300	0.01855	26245	2.6245E6	3.411E-3	0.7	2.2
45.008	300.0	5129.5	10000	20.0	4.225	135.008	408.2	600.0	0.6803	6724	13499.500	0.01868	26999	2.6999E6	3.411E-3	0.8	2.3
45.992	300.0	5165.3	10000	20.0	4.236	135.992	411.0	600.0	0.6851	6741	13753.100	0.01873	27506	2.7506E6	3.411E-3	0.8	2.3
47.012	300.0	5097.2	10000	20.0	4.224	137.012	405.6	600.0	0.6760	6722	14129.600	0.01867	28259	2.8259E6	3.411E-3	0.8	2.3
48.008	300.0	5152.2	10000	20.0	4.267	138.008	410.0	600.0	0.6834	6791	14380.800	0.01887	28762	2.8762E6	3.411E-3	0.8	2.3
48.992	300.0	5127.6	10000	20.0	4.151	138.992	408.0	600.0	0.6801	6606	14631.500	0.01835	29263	2.9263E6	3.411E-3	0.8	2.3
50.008	300.0	5095.7	10000	20.0	4.169	140.008	405.5	600.0	0.6758	6636	15007.400	0.01843	30015	3.0015E6	3.411E-3	0.8	2.3
51.012	300.0	5115.8	10000	20.0	4.233	141.012	407.1	600.0	0.6785	6737	15258.600	0.01871	30517	3.0517E6	3.411E-3	0.9	2.4
51.992	300.0	5079.7	10000	20.0	4.191	141.992	404.2	600.0	0.6737	6670	15511.300	0.01853	31023	3.1023E6	3.411E-3	0.9	2.4
53.008	300.0	5073.5	10000	20.0	4.159	143.008	403.7	600.0	0.6729	6619	15888.000	0.01838	31776	3.1776E6	3.411E-3	0.9	2.4
53.992	300.0	5130.6	10000	20.0	4.230	143.992	408.3	600.0	0.6805	6732	16139.800	0.01870	32280	3.2280E6	3.411E-3	0.9	2.4
55.008	300.0	5094.5	10000	20.0	4.170	145.008	405.4	600.0	0.6757	6636	16518.500	0.01843	33037	3.3037E6	3.411E-3	0.9	2.4
56.012	300.0	5107.8	10000	20.0	4.201	146.012	406.5	600.0	0.6774	6686	16766.600	0.01857	33533	3.3533E6	3.411E-3	0.9	2.4
57.004	300.0	5112.9	10000	20.0	4.214	147.004	406.9	600.0	0.6781	6707	17026.000	0.01863	34052	3.4052E6	3.411E-3	1.0	2.5
57.992	300.0	5119.7	10000	20.0	4.282	147.992	407.4	600.0	0.6790	6816	17394.900	0.01893	34790	3.4790E6	3.411E-3	1.0	2.5
59.004	300.0	5137.5	10000	20.0	4.182	149.004	408.8	600.0	0.6814	6656	17647.600	0.01849	35295	3.5295E6	3.411E-3	1.0	2.5
59.992	300.0	5098.5	10000	20.0	4.148	149.992	405.7	600.0	0.6762	6602	17897.500	0.01834	35795	3.5795E6	3.411E-3	1.0	2.5

Continuous ramp step 2

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

0.99600	296.6	4992.0	10000	20.0	4.210	151.996	397.3	593.3	0.6696	6700	280.5640	0.01903	561.13	56113	3.411E-3	0.0	2.5
1.9960	292.7	4902.4	10000	20.0	4.312	152.996	390.1	585.3	0.6665	6863	518.6200	0.02003	1037.2	1.0372E5	3.411E-3	0.0	2.5
3.0000	286.5	4697.3	10000	20.0	4.337	154.000	373.8	573.0	0.6523	6903	875.5140	0.02102	1751.0	1.7510E5	3.411E-3	0.1	2.6
4.0000	282.4	4540.8	10000	20.0	4.354	155.000	361.3	564.8	0.6398	6930	1114.8300	0.02172	2229.7	2.2297E5	3.411E-3	0.1	2.6
5.0120	276.4	4356.9	10000	20.0	4.438	156.012	346.7	552.7	0.6273	7064	1451.5100	0.02312	2903.0	2.9030E5	3.411E-3	0.1	2.6
6.0040	272.3	4260.9	10000	20.0	4.503	157.004	339.1	544.6	0.6226	7167	1678.1100	0.02416	3356.2	3.3562E5	3.411E-3	0.1	2.6
7.0000	268.1	4161.6	10000	20.0	4.544	158.000	331.2	536.2	0.6176	7232	1902.4399	0.02515	3804.9	3.8049E5	3.411E-3	0.1	2.6
8.0000	262.1	3973.8	10000	20.0	4.614	159.000	316.2	524.2	0.6032	7343	2222.8000	0.02672	4445.6	4.4456E5	3.411E-3	0.1	2.7
8.9960	258.1	3852.6	10000	20.0	4.692	159.996	306.6	516.2	0.5939	7467	2434.7000	0.02803	4869.4	4.8694E5	3.411E-3	0.1	2.7
10.012	251.9	3640.1	10000	20.0	4.677	161.012	289.7	503.8	0.5749	7443	2753.9600	0.02932	5507.9	5.5079E5	3.411E-3	0.2	2.7
10.988	247.9	3578.5	10000	20.0	4.796	161.988	284.8	495.7	0.5745	7634	2954.1101	0.03107	5908.2	5.9082E5	3.411E-3	0.2	2.7
12.016	241.8	3389.0	10000	20.0	4.802	163.016	269.7	483.6	0.5577	7643	3256.4900	0.03268	6513.0	6.5130E5	3.411E-3	0.2	2.7
13.004	237.6	3301.9	10000	20.0	4.848	164.004	262.8	475.3	0.5529	7716	3454.9399	0.03416	6909.9	6.9099E5	3.411E-3	0.2	2.7
13.996	233.5	3181.7	10000	20.0	4.896	164.996	253.2	467.0	0.5422	7792	3648.8799	0.03574	7297.8	7.2978E5	3.411E-3	0.2	2.7
14.996	227.5	3024.1	10000	20.0	4.931	165.996	240.7	454.9	0.5290	7849	3930.4700	0.03792	7860.9	7.8609E5	3.411E-3	0.2	2.8
16.008	223.3	2923.5	10000	20.0	4.945	167.008	232.6	446.6	0.5209	7870	4118.0698	0.03945	8236.1	8.2361E5	3.411E-3	0.3	2.8
16.996	217.1	2771.5	10000	20.0	5.020	167.996	220.6	434.1	0.5080	7989	4393.2500	0.04239	8786.5	8.7865E5	3.411E-3	0.3	2.8
18.000	213.0	2683.8	10000	20.0	5.045	169.000	213.6	426.1	0.5012	8030	4568.4399	0.04423	9136.9	9.1369E5	3.411E-3	0.3	2.8
19.000	208.9	2581.8	10000	20.0	5.104	170.000	205.5	417.9	0.4917	8123	4744.2798	0.04652	9488.6	9.4886E5	3.411E-3	0.3	2.8
20.000	202.7	2451.7	10000	20.0	5.164	171.000	195.1	405.4	0.4812	8219	5000.0698	0.05000	10000	1.0000E6	3.411E-3	0.3	2.9
21.004	198.7	2349.2	10000	20.0	5.191	172.004	186.9	397.4	0.4705	8262	5162.5098	0.05233	10325	1.0325E6	3.411E-3	0.4	2.9
21.996	192.5	2219.1	10000	20.0	5.245	172.996	176.6	385.0	0.4586	8347	5407.1299	0.05631	10814	1.0814E6	3.411E-3	0.4	2.9
23.000	188.3	2118.0	10000	20.0	5.266	174.000	168.5	376.6	0.4476	8381	5568.8901	0.05910	11138	1.1138E6	3.411E-3	0.4	2.9
23.996	184.2	2034.3	10000	20.0	5.314	174.996	161.9	368.4	0.4394	8457	5796.5698	0.06230	11593	1.1593E6	3.411E-3	0.4	2.9
25.000	178.1	1910.2	10000	20.0	5.325	176.000	152.0	356.1	0.4268	8474	5943.9502	0.06681	11888	1.1888E6	3.411E-3	0.4	2.9
25.996	173.8	1833.8	10000	20.0	5.351	176.996	145.9	347.7	0.4197	8516	6093.9502	0.07045	12188	1.2188E6	3.411E-3	0.4	2.9
26.988	167.8	1708.3	10000	20.0	5.410	177.988	135.9	335.6	0.4051	8610	6300.2202	0.07645	12600	1.2600E6	3.411E-3	0.4	3.0
27.996	163.7	1631.0	10000	20.0	5.416	178.996	129.8	327.3	0.3965	8619	6437.5898	0.08044	12875	1.2875E6	3.411E-3	0.5	3.0
29.000	159.5	1553.1	10000	20.0	5.457	180.000	123.6	318.9	0.3875	8685	6574.9399	0.08539	13150	1.3150E6	3.411E-3	0.5	3.0
30.004	153.2	1449.5	10000	20.0	5.487	181.004	115.3	306.5	0.3764	8733	6768.5898	0.09298	13537	1.3537E6	3.411E-3	0.5	3.0
31.004	149.1	1365.2	10000	20.0	5.514	182.004	108.6	298.3	0.3642	8775	6893.3599	0.09863	13787	1.3787E6	3.411E-3	0.5	3.0
32.008	142.8	1253.8	10000	20.0	5.547	183.008	99.77	285.6	0.3493	8829	7080.5601	0.1082	14161	1.4161E6	3.411E-3	0.5	3.1
33.000	138.5	1177.7	10000	20.0	5.564	184.000	93.72	277.0	0.3383	8856	7199.9302	0.1154	14400	1.4400E6	3.411E-3	0.6	3.1
34.012	134.5	1118.5	10000	20.0	5.606	185.012	89.01	268.9	0.3310	8923	7311.3599	0.1234	14623	1.4623E6	3.411E-3	0.6	3.1
35.004	128.1	1028.5	10000	20.0	5.634	186.004	81.84	256.2	0.3195	8967	7479.6899	0.1367	14959	1.4959E6	3.411E-3	0.6	3.1
36.004	123.8	964.97	10000	20.0	5.646	187.004	76.79	247.6	0.3102	8985	7585.7100	0.1466	15171	1.5171E6	3.411E-3	0.6	3.1
37.004	119.7	903.14	10000	20.0	5.673	188.004	71.87	239.5	0.3001	9029	7737.6699	0.1574	15475	1.5475E6	3.411E-3	0.6	3.1
38.020	113.4	809.55	10000	20.0	5.694	189.020	64.42	226.8	0.2841	9062	7835.3101	0.1762	15671	1.5671E6	3.411E-3	0.6	3.2
39.004	109.0	746.24	10000	20.0	5.710	190.004	59.38	217.9	0.2725	9088	7934.5400	0.1914	15869	1.5869E6	3.411E-3	0.7	3.2
40.016	104.8	692.49	10000	20.0	5.728	191.016	55.11	209.5	0.2630	9116	8021.6802	0.2076	16043	1.6043E6	3.411E-3	0.7	3.2
41.008	98.40	612.07	10000	20.0	5.753	192.008	48.71	196.8	0.2475	9156	8152.3198	0.2364	16305	1.6305E6	3.411E-3	0.7	3.2
42.000	93.92	562.32	10000	20.0	5.777	193.000	44.75	187.8	0.2382	9194	8239.3799	0.2606	16479	1.6479E6	3.411E-3	0.7	3.2
43.008	89.74	511.10	10000	20.0	5.774	194.008	40.67	179.5	0.2266	9190	8313.9297	0.2853	16628	1.6628E6	3.411E-3	0.7	3.2
44.000	83.34	453.87	10000	20.0	5.802	195.000	36.12	166.7	0.2167	9235	8426.0000	0.3324	16852	1.6852E6	3.411E-3	0.7	3.3
45.004	78.79	402.94	10000	20.0	5.816	196.004	32.07	157.6	0.2035	9256	8500.0303	0.3728	17000	1.7000E6	3.411E-3	0.8	3.3
46.020	74.59	359.97	10000	20.0	5.829	197.020	28.65	149.2	0.1920	9278	8562.0703	0.4169	17124	1.7124E6	3.411E-3	0.8	3.3
46.996	70.35	324.94	10000	20.0	5.834	197.996	25.86	140.7	0.1838	9286	8624.0098	0.4691	17248	1.7248E6	3.411E-3	0.8	3.3
47.996	65.85	282.08	10000	20.0	5.844	198.996	22.45	131.7	0.1704	9300	8685.8701	0.5362	17372	1.7372E6	3.411E-3	0.8	3.3
48.996	59.25	236.87	10000	20.0	5.859	199.996	18.85	118.5	0.1591	9325	8766.2002	0.6642	17532	1.7532E6	3.411E-3	0.8	3.3
50.000	54.96	203.80	10000	20.0	5.866	201.000	16.22	109.9	0.1475	9336	8815.8301	0.7726	17632	1.7632E6	3.411E-3	0.8	3.4
51.000	50.33	171.34	10000	20.0	5.873	202.000	13.63	100.7	0.1355	9347	8865.2305	0.9226	17730	1.7730E6	3.411E-3	0.9	3.4
52.000	45.57	141.78	10000	20.0	5.882	203.000	11.28	91.14	0.1238	9362	8907.7598	1.127	17816	1.7816E6	3.411E-3	0.9	3.4
52.996	39.11	110.49	10000	20.0	5.891	203.996	8.793	78.22	0.1124	9376	8962.8896	1.533	17926	1.7926E6	3.411E-3	0.9	3.4
53.992	34.17	85.624	10000	20.0	5.897	204.992	6.814	68.34	0.09970	9386	8999.6104	2.010	17999	1.7999E6	3.411E-3	0.9	3.4
55.000	28.95	64.712	10000	20.0	5.899	206.000	5.150	57.91	0.08893	9388	9029.5996	2.800	18059	1.8059E6	3.411E-3	0.9	3.4
56.000	24.46	47.115	10000	20.0	5.901	207.000	3.749	48.92	0.07665	9392	9053.7002	3.925	18107	1.8107E6	3.411E-3	0.9	3.5
57.008	21.90	38.708	10000	20.0	5.902	208.008	3.080	43.79	0.07033	9394	9065.5596	4.898	18131	1.8131E6	3.411E-3	1.0	3.5
58.000	15.73	21.603	10000	20.0	5.905	209.000	1.719	31.46	0.05465	9397	9088.5303	9.495	18177	1.8177E6	3.411E-3	1.0	3.5
58.996	10.37	10.141	10000	20.0	5.906	209.996	0.8070	20.73	0.03892	9400	9099.9004	21.87	18200	1.8200E6	3.411E-3	1.0	3.5
60.004	7.295	4.7059	10000	20.0	5.908	211.004	0.3745	14.59	0.02567	9402	9104.9902	44.17	18210	1.8210E6	3.411E-3	1.0	3.5

